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Dual acquisition magic-angle spinning solid-state NMR-spectroscopy: simultaneous acquisition of multidimensional spectra of biomacromolecules. Angew Chem Int Ed Engl 2012 Mar 12;51(11):2731-5

Date

02/09/2012

Pubmed ID

22311700

Pubmed Central ID

PMC3513283

DOI

10.1002/anie.201108132

Scopus ID

2-s2.0-84858058799 (requires institutional sign-in at Scopus site)   74 Citations

Abstract

Fast data collection: a general method for dual data acquisition of multidimensional magic-angle spinning solid-state NMR experiments is presented. The method uses a simultaneous Hartmann-Hahn cross-polarization from (1)H to (13)C and (15)N nuclei and exploits the long-living (15)N polarization for parallel acquisition of two multidimensional experiments.

Author List

Gopinath T, Veglia G

Author

Gopinath Tata PhD Assistant Professor in the Biophysics department at Medical College of Wisconsin




MESH terms used to index this publication - Major topics in bold

Carbon Isotopes
Hydrogen
Macromolecular Substances
Nitrogen Isotopes
Nuclear Magnetic Resonance, Biomolecular
Ubiquitin